Download PDF by F. Marott Sinex (auth.), Seymour Rothchild (eds.): Advances in Tracer Methodology: Volume 1

By F. Marott Sinex (auth.), Seymour Rothchild (eds.)

ISBN-10: 1468486195

ISBN-13: 9781468486193

ISBN-10: 1468486217

ISBN-13: 9781468486216

The 5 Symposia on Advances in Tracer method have been held every year from 1957 to 1961. The symposia have been directed to scientists who're energetic in using tracer ideas to assist clear up their medical difficulties. The structure, a casual one-day assembly which include approximately ten papers and shutting with a cocktail hour, fostered an energetic trade of data between audio system and viewers. even though the 1st symposia have been constrained to using tritium as a tracer isotope, the bigger function of the conferences used to be to disseminate details in terms of the complete isotopic tracer box. The sponsoring businesses, all actively engaged in promoting items within the nuclear box, tried to supply a noncom­ mercialized discussion board which might facilitate this alternate of in­ formation. the gathering of papers provided herein represents many of the talks offered on the first symposia plus a number of applicable papers that have seemed both in Atomlight, the bulletin of the hot England Nuclear Corp., or that have been submitted without delay for inclusion during this assortment. even supposing all the authors used to be given the chance to revise his paper, it's most probably that many of the thoughts or instrumentation defined may well have already got been superseded by means of contemporary improvements.

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Chern. and Ind. (London) 1165 (1961). (6) Wallings, Briggs, Cummings, and Mayo. j. Am. Chern. Soc. 72, 48 (1950). (7) Shores and Moser. j. Phys. Chern. 65, 570 (1961). (8) Nystrom and Rajan. Unpublished results. (9) Dutton, jones, Davison, and Nystrom. 140th National Meeting of the American Chemical Society, Chicago, Illinois, September 3-8, 1961. (10) jones, Mason, Dutton, and Nystrom. j. Org. Chern. 25, 1413 (1960). (11) Whisman. Anal. Chern. 33, 1284 (1961). (12) Sato and Takahashi. Bull. Chern.

1) and after chemical purification (Fig. 2) differ sharply from those of the saturated esters in that the major radioactive peaks precede the peaks for methyl oleate. This is not an isotope effect, as was reported for cyclohexane-d12 by Wilzbach [9], but rather is a result of saturation of the double bond to give methyl stearate-H3. After converting tritiated methyl oleate to oleic acid, the latter was cleaved at the carbon-carbon double bond by periodate-permanganate oxidation [8]. The products were analyzed by partition chromatographic analysis.

Peak corresponding to 6-deoxy-D-glucose on a control chromatogram. B. peak suspected to contain incompletely deacetylated acetyl-6-deoxyD-glucose. 34 The Tritium Gas Exposure Method 10 8 (f) o z <{ (f) 6 ::> o I I- 4 ~ ~ ~ 2 10 20 CENTIMETERS FROM 30 ORIGIN 40 Fig. 2. 6-deoxy-D-glucose after chromatographic purification. dissolved in a small volume of water and applied as a band to sheets of Whatman number 3 filter paper. Ten to a dozen sheets were used for each compound. The sheets were then developed in a butanol-pyridine-water (6: 4: 3) solvent [7].

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Advances in Tracer Methodology: Volume 1 by F. Marott Sinex (auth.), Seymour Rothchild (eds.)


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